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OH OH ~ ¥¥ 160 1<0 120 160 Fig. 6. 100 80 60 <0 20 100 80 60 <0 20 13c 160 1<0 120 100 80 60 W 20 NMR spectra of a linear dimer, trimer, tetramer, and a cyclic tetramer. 5 ppm region, arising from the hydrogens on the bridging methylene groups, provides a most useful aspect of the lR NMR spectra of the calixarenes. The apparent identity in this region between the calix- and calixarenes with respect to the spectral pattern and coalescence temperature (eQ 48°C in CRCl 3 for the change from a pair of doublets to a singlet) caused confusion for some years.
D. Morgan, K. T. Potts, and R. J. W. Rees: Tetrahedron 29, 1659 (1973). V. Bocchi, D. Foina, A. Pochini, R. Ungaro, and G. D. Andreetti: Tetrahedron 38, 373 (1982). J. Vicens, T. Pilot, D. Gamet, R. Lamartine, and R. R. Acad. Sc. Paris 302, II, 15 (1986). Z. Asfari and J. Vicens: Makrornol. , Rapid Cornrnun. 10, 181 (1989). A. Zinke, R. Kretz, E. Leggewie, and K. Hassinger: Monatsh. 83, 1213 (1952). C. D. Gutsche and P. F. Pagoria: J. Org. Chern. 50, 5795 (1985). Jpn. A. , 101: 191411w). S. I. Chen: Ph.